Introduction and preparation of 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2

2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2 is a white or off-white crystal. It is used as an intermediate in the synthesis of medicines and pesticides and is used in the synthesis of 2-diazoacetoacetate-p-nitrobenzyl ester, etc.

Here is the content list:

• What is 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2?

• How is 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2 formulated?

• About Mulei

What is 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2?

English name: o-Bromovalerophenone

English alias: 2-Bromo- 1-phenylpentan-1-one

CAS number: 49851-31-2

Molecular formula: C11H13BrO

Molecular weight: 241.12400

Appearance: 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2 is usually a yellow liquid.

Purity: 98%

Density: 1.31g/cm3

Boiling point: 282.267oC at 760 mmHg

Flashpoint: 42.513oC

Refractive index: 1.541

How is 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2 formulated?

At room temperature, add 16.2 g (0.1 mol) valerophenone and 30.9 g (0.3 mol) sodium bromide to a 500 mL round-bottomed flask, stir well, then add 24 g (0.2 mol) 30% hydrochloric acid, slowly drop Add 19 g (0.15 mol) of 30% hydrogen peroxide, and continue to react for 1 to 2 h. After TLC monitoring is completed, stop stirring, let stand for stratification, and use saturated sodium carbonate and saturated brine respectively. After washing, the organic phases were combined, concentrated, and dried over anhydrous magnesium sulfate to obtain 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2 as a bright yellow oily liquid with a yield of 95% and a purity of 98 % (HPLC method).

About Mulei

Mulei (Wuhan) New Material Technology Co. Ltd is a technology-based company specializing in organic intermediates, pharmaceutical intermediates, chemical solvents, and agrochemical products, integrating R&D, production, and trade of chemical intermediates. We manufacture and supply 2-Bromo-1-phenyl-1-pentanone CAS: 49851-31-2, phenacetin fluffy powder, phenacetin crystals, alpha bromobenzophenone, valerophenone, watermelon ketone, and cool chloride, etc. Looking forward to working with you. We ensure strong product development capabilities. We have established a laboratory center at Yantai University. The core technology system with independent intellectual property rights has been rated as the "Hubei Enterprise Technology Center". So far, we have 35 proprietary technologies and 15 patents, including 4 invention patents and 11 utility patents. We are a national high-quality supplier.

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